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Chapter 5

demulsifier PR5 prepared as described in section 5.3.1. In the figure samples 2
and 3 have clearer aqueous phases than others. Sample 2 has more separated

free water and thinner rag layer. So sample 2 with silicate at initial pH 8.5 has the

best emulsion separation.

Control PRi PR2 PR3 PR4 PR5 PR5


Figure 5.1 24 h emulsion adding 200 ppm demulsifier PRi - PR5 at 50 0C


Sample: 12      3

Adding:        Na2SiOs    NaOH

I. pH:     8.3       8.5          8.5

E. pH:   8.0    8.0-8.5    8.0-8.5

4

Na2SiOs

8.8

8.5


5          6

NaOH Na2SiO3SNaOH

8.8         8.8

8.5         8.5


Figure 5.2 Photographs of 24 h emulsion with 200 ppm PR5 adding NaOH or
Na2SiO3 at different pH

151



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