Synthesis and biological activity of α-galactosyl ceramide KRN7000 and galactosyl (α1→2) galactosyl ceramide



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Veerapen et al.

Page 11


Scheme 3.

Reagents and conditions: (a) PhSH, DMF, Cs2CO3, 75%; (b) (CH3)2Si(Cl)2, Pyridine,
CH2Cl2, quant; (c) 5, Pyridine, DMF, 72%; (d) NIS, CH3NO2, 66%; (e) NaOMe/MeOH, quant;

(f) H2, Pd/C, MeOH, 80%; (g) C25H51COCl, THF, NaOAc, 75%.

Published as: BioorgMed Chem Lett. 2009 August 01; 19(15): 4288-4291.



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